Analytical Testing
The Environmental Chemistry Laboratory coordinates closely with its departmental programs to enforce California’s hazardous substances and hazardous waste laws and regulations. It receives and analyzes samples collected by field staff from the different programs, such as Hazardous Waste Management Program, Cleanup and Safer Consumer Products. The environmental samples come from different sites and industries and from various special projects and initiatives of the Department. The Laboratory also receives and analyzes biological samples from other entities such as Center for Disease Control and Prevention (CDC) and California Department of Public Health (CDPH).
The Berkeley and Pasadena laboratories are equipped with cutting edge analytical instruments that can measure hundreds of chemicals in a wide range of matrices. The laboratories follow standard methods issued by authoritative bodies such as the US EPA, but the laboratories also adapt and develop new methods to measure new, emerging contaminants or known contaminants in new matrices (e.g. children’s toys, e-waste, carpets, fabrics).
In its analytical testing approach, the Laboratory examines each matrix with its unique attributes and determines the appropriate sample pre-preparation technique(s), sample preparation technique(s) such as digestion or extraction and cleanup procedures and analytical method. ECL scientists have the experience and expertise to analyze difficult matrices that commercial laboratories cannot handle. The goal of the Laboratory is to produce analytical results that are scientifically valid, meaningful and defensible in legal proceedings in support of the Department and State.
Our staff are devoted to providing thorough quality control to produce high-quality data. Occasionally time constraints arise when requests fall outside our scope or exceed our workflow capacity. In these cases, we use commercial labs to address overflow and out of scope requests such as Asbestos or Fish Bioassays. Commercially produced data adheres to the same data quality standards as if it were produced by ECL. In-house analysis is prioritized for samples likely to be used in legal proceedings or legislative decision-making.
ECL Analytical Testing Capabilities Overview
ECL analytical testing capabilities are summarized below:
Analytical Testing | ||
---|---|---|
Matrices | Solid | soil, human tissue, vegetation, wood, electronic-wastes, plumbing fixtures, brake pads, jewelry, glass beads, glass bottles, plastic packaging, auto shredder wastes, plastic toys, house dust, children's foam products, hand wipes |
Liquid | water, sludges, oil, blood, serum, breast mik, urine | |
Gas | indoor air, soil gas | |
Sample Preparation | Pre-prep | drying, sieving, cleaning, grinding, dismantling, cutting, scraping, drilling, sawing and dry freezing |
Prep | microwave digestion, acid digestion, Waste Extraction Test (WET), Toxicity Characteristic Leaching Procedure (TCLP), Soxhlet extraction, Soxhtherm extraction, separatory funnel liquid-liquid extraction (SFLLE), purge and trap extraction, sonication, solid phase extraction (SPE) and accelerated solvent extraction (ASE) |
ECL Berkeley Analytical Testing Capabilities
ECL Berkley A2LA accredited serum samples, consumer products, sediment, soil, waste, and hazardous waste analyses:
Test/Technology | Referenced Method |
---|---|
California Waste Extraction Test (WET)* | CCR TITLE 22 |
Flashpoint | ASTM D3278-78 |
EPA 1020B | |
Mercury Analysis by Flow Injection Mercury System | EPA 7471B |
EPA 7470A | |
Mercury Analysis by Thermal Decomposition Amalgamation, Atomic Absorption Spectroscopy | EPA 7473 |
Metal Analysis by ICP-OES* | EPA 6010C |
PCBs by GC/ECD* | EPA 8082A |
pH Determination of Solid & Liquid Wastes | EPA 9045D |
EPA 9040C | |
Toxicity Characteristics Leaching Procedure (TLCP)* | EPA 1311 |
Hexavalent Chromium (CrVI), colorimetric by Spectrophotometer | EPA 7196A |
Polychlorinated Dibenzo-p-Dioxins and Polycho Dibenzofurans by HRGC/HRMS* | EPA 1613 (October 1994) |
Polyfluoroalkyl Chemicals (PFAS) by online SPE-HPLC-TIS-MS/MS* | Centers for Disease Control and Prevention (CDC) Method 6304.05 |
Organophosphate and Brominated Flame Retardants by GC-Tandem MS* | In house method validated |
Screening Consumer Products by X-Ray Fluorescence Spectrometry (XRF)* | In house method validated |
Volatile Organic Compounds by Purge & Trap, GC-MS* | EPA 5030C |
EPA 5035A | |
EPA8260C |
*Click to open list of target analytes
ECL Pasadena Analytical Testing Capabilities
ECL Pasadena A2LA accredited sediment, soil, waste, and hazardous waste analyses:
Target | Reference Method |
---|---|
1,4-Dioxane by Solid Phase Microextraction (SPME) GC/QQQ | In-house |
California Waste Extraction Test (WET) Metals and Mercury* | CCR TITLE 22 |
EPA 6010D | |
EPA 7470A | |
Carbofuran by GC/QQQ | EPA 3540C (Modified) |
EPA 8270E | |
Flashpoint | ASTM D3278-78 |
EPA 1020B | |
Gas Range Organics (GRO) by Purge & Trap GC-FID | EPA 5030C, 5035A |
EPA 8015D | |
Hexavalent Chromium in Water by HPLC ICP-MS/MS | EPA 6020B (Modified) |
Mercury Analysis by Flow Injection Mercury System | EPA 7470A |
EPA 7471B | |
Methamidophos | In-house |
pH Determination of Solid and Liquid Wastes | EPA 9045D |
EPA 9040C | |
Toxicity Characteristic Leaching Procedure (TCLP) of Metals and Mercury* | EPA 1311 |
EPA 6010D | |
EPA 7470A |
*Click to open list of target analytes
ECL Pasadena Analytical Testing Capabilities – Flexible Scope
ECL Pasadena A2LA accredited flexible scopes adhering to A2LA P112:
Flexible Scope Analytes | Technique |
---|---|
1,4 Dioxane | Purge and Trap GC/MS and GC/QQQ |
Copper in Seawater | ICP-MS/MS |
Diesel and Motor Oil Range Organics (DRO and MORO) | GC FID |
Metals Analysis | ICP OES |
Organochlorine Pesticides | GC/QQQ |
Organophosphorous Pesticides | GC/QQQ |
Polychlorinated Biphenyls (PCBs) | GC/QQQ |
Pesticides in Wastewater | GC QTOF |
LC MS/MS | |
Per- and Polyfluorinated Alkyl Substances (PFAS) | LC MS/MS |
Polycyclic Aromatic Hydrocarbons (PAHs) | GC/QQQ |
Volatile Organics | Purge and Trap GC/MS and GC/QQQ |
Volatile Organics | GC/MS |
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